Table 4 Crystallographic data and refinement statistics for PBD ID 4EO5

Data collection statistics

Space group

P3₁21

Resolution (Å)

37.24 to 2.30 (2.38 to 2.30)

Unit cell dimensions (Å)

97.69, 97.69, 115.07

Observed reflections

147,637

Unique reflections

28,711

Completeness (%)

100 (100)

Redundancy

5.14 (5.18)

R_merge^a (%)

9.0 (47.4)

< I/σ >

8.4 (2.4)

Refinement statistics

Resolution range (Å)

15 to 2.35 (2.41 to 2.35)

R value (%)

20.4 (28.9)

Free R value (%)

24.2 (36.7)

Number of reflections used

25,471

Luzatti coordinate error (Å)

0.33

Average B factor main chain (Ų)

25.93

Root mean square deviation from ideality

Bond angle (˚)

1.282

Bond length (Å)

0.013

Solvent atoms

169

Protein atoms

2844